BEAMLINE GUIDE
NSLS II NYX (19-ID)
National Synchrotron Light Source NSLSII
Upton, New York
Irelec ISARA2
The NYX beamline has the scientific objective of providing a state-of-the-art source for a wide spectrum of crystallographic experiments and a cutting-edge source for optimized anomalous diffraction experiments. While moving to incorporate microbeams, we also want to preserve the versatility of optimized anomalous scattering experiments across a broad spectrum of atomic resonances from different elements. In order to carry out these experiments and research, we capitalize on the intrinsic brightness of NSLS-II to optimize anomalous signals by improving energy resolution.
NYX has an energy range from 7-14 keV with a 25 μm FWHM spot size.
The sample mounting robot is an ISARA2 from Irelec which provides a typical sample exchange time near 15 seconds. The robot will only accept UniPuck V1 pucks with either SPINE or ALS bases. We recommend SPINE bases to conform to other NSLS-II beamline requirements.
The detector at NYX is an Eiger2 9M XE. Data can be transferred via Globus.
Data collection can be done in-person or remotely through NX. The data collection software is LSDC which is used at the other NSLS-II beamlines.
Contacts
Kevin Battaile
Other Links
Tools
We recommend the following tools for their compatibility and ease-of-use.
** Use MiTeGen Reusable bases only with MiTeGen brand loops/mounts. If using other mounts, use glue-in style bases.**
Recommended | Accepted* | |
---|---|---|
Puck Style | Uni-Puck | Uni-Puck |
Mount/Loop Style | MicroMounts™ & MicroLoops™ LD | Any |
Rod Length | 18mm/SPINE | 18mm/SPINE |
Base Style | SPINE (B5) | SPINE (B5-Reusable), SPINE (B5), B1 (ALS) |
Sample Preparation Kits
Convenient kits of compatible assemblies of MiTeGen recommended products
Beamline Sample Preparation Kits are available in 3 aperture size assortments based on your crystal sizes and include:
- Assemblies of 100 Crystal Mounts, on 18 mm pins, available in the following assortment:
- 20 x Dual-Thickness MicroLoops ™ LD (5 each of 10, 20, 30 and 50 μm aperture sizes)
- 40 x Dual-Thickness MicroMount ™ (10 each of 75, 100, 150 and 200 μm aperture sizes)
- 20 x Dual-Thickness MicroLoops ™ (5 each of 300, 400, 500 and 600 μm aperture sizes)
- 20 x MicroMeshes ™ (5 each of 10, 25, 50 and 25L μm aperture sizes)
- Installed in 100 B5-R reusable bases or 100 regular bases
- Packaged and stored in 5 MiTeGen base holders
Uni-puck Starter Kit 2 includes:
- (7) Universal V-1 Pucks
- (1) Double Puck Loading Dewar with Lid
- (1) Puck Wand
- (1) Puck Dewar Loading Tool
- (1) Puck Separator Tools
- (1) Shelved Puck Shipping Cane
- (1) Bent Cryo-Tong
- (1) Cryo Express Dry Shipper (CX100)
- (1) Shipping case for CX100
*custom kits are available, contact MiTeGen with specific requests.
Order Beamline Kits
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Small Aperture Assortment Beamline Sample Preparation Kit
100 Dual Thickness MicroMounts™ (25 each of 10, 20, 30 and 50 μm aperture DT MicroMounts™) On standard... -
Medium Aperture Assortment Beamline Sample Preparation Kit
100 Dual Thickness MicroMounts™ (25 each of 75, 100, 150 and 200 μm aperture DT MicroLoops™) On standard... -
Large Aperture Assortment Beamline Sample Preparation Kit
100 Dual Thickness MicroLoops™ (25 each of 300, 400, 500 and 600 μm aperture DT MicroLoops™) On standard... -
Universal Puck (Uni-Puck) Starter Kits
To get you up–and–running sending samples to the beamline in easy-to-order bundles. Full Description